In order to fit the thermo-mechanical stability domain of tubes on specifications, 3 thermal cycles have been tested, regarding to relaxation of internal stress and changes in macroscopic thermo-mechanical properties. Experimental expansion curves and microstructure observation show that thermal treatments permitts such a good fitting. For a better understanding of physical internal phenomena, internal stress has been measured by neutron diffraction on tube samples after each thermal treatment. Results show a significant decrease of stress due to cycling in cold temperature. In order to decrease the absolute value of CTE of assemblies, a new concept of thermo-mechanical stable linkage has been developped, which consists in a common alumlinum infiltration of superposed carbon preforms. Structural bonding, which usually affects stability properties and impose surface treatments and polymerization, can so be avoided. The study has been achieved through CNES (Centre National d’Etudes Spatiales) and French Ministry of Defense (DGA) supports. |