CdS nanocrystalline were prepared by precipitation from a mixture of aqueous solutions of cadmium salts and sulfur salts without adding any surface-termination agent. Their crystal structures and particle sizes were determined by X-ray diffraction (XRD). The CdS nanocrystalline precipitated from different precursors exhibited three cases: cubic phase, hexagonal phase and a mixture of cubic and hexagonal phases. The photoluminescence (PL) of cadmium salt precursors and CdS nanocrystalline is also analyzed. Similar spectral band structure of cadmium salt precursors and CdS nanocrystalline is found. The spectral intensity of the CdS-Cd rich and CdS-S rich nanocrystalline shows that the precursors themselves have important effect on the PL of CdS nanocrystalline.
A new technique of reducing surface roughness of photoresist grating is presented. In this paper, photoresist melting method, which is low-cost, short-period and easy realization, is presented. In addition, the influence of photoresist melting on the groove profile of the photoresist grating is investigated. Experimental results show that the surface roughness reduces due to surface tension, when developed photoresist is heated to be melting state by this method. In experiment, when the melted photoresist grating is etched by ion beam, the surface relief grating possessing preferable groove profile is obtained on K9 glass substrate, then the surface is evaporated by aluminum using vacuum evaporation, holographic grating with preferable groove profile is successively fabricated.
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